Method for preparing magnetic iron oxide
US9315392B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | May 21, 2012 |
| Grant date | Apr 19, 2016 |
| Priority date | — |
| Expiry date | May 21, 2032 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC01P2006/42
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
A method for preparing magnetic iron oxide Fe21.333O32, comprising the following steps: (1) preparing a ferrous salt solution with solid soluble ferrous salt; (2) preparing a hydroxide solution; (3) mixing said hydroxide solution and said ferrous salt solution in a co-current manner for reaction at an alkali ratio of 0.6-0.8 and a reaction temperature not exceeding 30° C.; (4) after the reaction in step (3) is finished, yielding a first mixture, then charging said first mixture with a gas containing oxygen for oxidation, and controlling the first mixture at a pH value of 6-8 until the oxidation is finished to yield a second mixture; (5) filtering, washing with water and drying said second mixture obtained in step (4) to yield a precursor; and (6) calcining the precursor obtained in step (5) at 250-400° C.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.