Patent · US Active

Method for manufacturing optically active carboxylic acid ester

US9315442B2 · kind B2 · utility

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19Claims
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Key dates

Filing dateJun 7, 2012
Grant dateApr 19, 2016
Priority date
Expiry dateJun 11, 2032

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C2603/26
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A method that manufacturers an optically active carboxylic acid ester at high yield and high enantioselectivity is provided. An optically active carboxylic acid ester is manufactured at high yield and high enantioselectivity by reacting a racemic carboxylic acid and a specific alcohol or phenol derivatives in a polar solvent having a dipole moment of 3.0 or higher in the presence of an acid anhydride and an asymmetric catalyst, esterifying one enantiomer of the racemic carboxylic acid at high selectivity, and increasing the amount of esterified carboxylic acid by racemizing the optically active carboxylic acid which is the other enantiomer not used in esterification.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.