Method for the manufacture of phosphonoalkyl iminodiacetic acid
US9315528B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Oct 27, 2010 |
| Grant date | Apr 19, 2016 |
| Priority date | — |
| Expiry date | Oct 27, 2030 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07F9/3808
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
An improved method for the manufacture of phosphonoalkyl iminodiacetic acid M2PO3—X—N—(CH2COOM)2 wherein X is a C1-6 linear or branched alkyl group; and M is selected from hydrogen, alkali, earth-alkali, ammonium and protonated amine is disclosed. The iminodiacetic acid starting material is reacted with a substantially stoichiometric amount of phosphorous acid, in the presence of a large excess of phosphoric acid to thereby yield a reaction medium insoluble reaction product (PAI-DA) which can be separated from the reaction medium. In a particularly preferred approach, the phosphorous acid is prepared in situ starting from liquid P4O6.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.