Manufacture of methylolalkanes
US9394218B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Jul 23, 2014 |
| Grant date | Jul 19, 2016 |
| Priority date | — |
| Expiry date | Jul 23, 2034 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01J2219/24
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A multistage tubular reaction system and method for preparing methylol derivatives of an aldehyde includes a tubular reaction system with a plurality of successive reactor stages provided with a formaldehyde containing feed stream. The system includes multiple feed ports for the staged addition of C2 or higher condensible aldehyde and/or base to the formaldehyde containing stream at a plurality of successive feed points to provide a production stream, which is progressively provided with additional reactants as the production stream advances through the successive reaction stages. Advantages include better temperature control and reduced byproduct formation.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.