Process for producing silica-comprising polyol dispersions and their use for producing polyurethane materials
US9403932B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Oct 8, 2009 |
| Grant date | Aug 2, 2016 |
| Priority date | — |
| Expiry date | Jul 25, 2032 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC01P2006/82
- WIPO fieldBasic materials chemistry
- WIPO sectorChemistry
Abstract
Provided is a process for producing silicate-comprising polyols, comprising (i) admixing an aqueous silica sol (K) having an average particle diameter 1-150 nm, silica content 1-60% by weight and a pH of 1-6, with a 0.1- to 20-fold amount of at least one organic solvent (L), (ii) admixing the resulting mixture with a polyol, (iii) removing at least partially water and the organic solvent (L) by distillation, (iv) admixing with 0.1-30 mol % of at least one compound (S) which has at least one at least monoalkoxylated silyl group and at least an alkyl, cycloalkyl or aryl substituent, which may contain heteroatoms, wherein the substituent optionally contains a group reactive toward an alcohol, an amine or an isocyanate, and (v) optionally adjusting the pH of the silicate-comprising polyol to 7-12 by addition of a basic compound.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.