Process for producing polyurethane resin
US9464154B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Nov 1, 2013 |
| Grant date | Oct 11, 2016 |
| Priority date | — |
| Expiry date | Nov 1, 2033 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC08G2120/00
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
A process for producing a polyurethane resin of the present invention includes a step (i) of obtaining a prepolymer by adding an alcohol (B) to isocyanate (A) such that a ratio of hydroxyl groups to isocyanato groups of the isocyanate (A) falls into a range of 10 mol % to 20 mol % and reacting the isocyanate (A) with the alcohol (B) in the presence of an acidic phosphoric acid ester (C) and a hindered amine-based compound (D), a step (ii) of obtaining a polymerizable composition in a manner in which the alcohol (B) is further added to and mixed with the prepolymer at a temperature of equal to or less than 30° C., and a step (iii) of polymerizing the prepolymer and the alcohol (B) contained in the polymerizable composition. The isocyanate (A) contains an aromatic isocyanate and the alcohol (B) has two or more hydroxyl groups and is further defined.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.