Preparation method of polycyclohexylenedimethylene terephthalate resin having excellent color, and polycyclohexylenedimethylene terephthalate resin prepared by the same
US9487623B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Sep 24, 2013 |
| Grant date | Nov 8, 2016 |
| Priority date | — |
| Expiry date | Sep 24, 2033 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC08G63/85
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
A preparation method of a polycyclohexylenedimethylene terephthalate resin according to the present invention includes the steps of injecting a titanium compound and a germanium compound as catalysts to a mixture of a diol compound and dicarboxylic acid under stirring and performing esterification reaction and polycondensation reaction, in which the titanium compound is injected in a titanium atom content of 20 ppm or less, based on the weight of the final polycyclohexylenedimethylene terephthalate resin. The preparation method of the polycyclohexylenedimethylene terephthalate resin according to the present invention can be used to prepare a polycyclohexylenedimethylene terephthalate resin that has excellent degree of polymerization, color and light reflectance and has remarkably improved heat stability, and it is suitable to use the polycyclohexylenedimethylene terephthalate resin according to the present invention as an LED housing material.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.