Patent · US Active

Process for producing sulfuric acid with low levels of niter

US9499405B2 · kind B2 · utility

4Cited by
2References
26Claims
0Family size

Assignee

Inventor

Key dates

Filing dateMar 10, 2015
Grant dateNov 22, 2016
Priority date
Expiry dateMar 12, 2035

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01B17/90
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

This disclosure relates to a process for producing sulfuric acid with reduced levels of niter. The process involves (a) providing an absorption tower wherein sulfur trioxide is absorbed in a sulfuric acid feed having a first sulfuric acid solution to produce a sulfuric acid effluent having (i) a second sulfuric acid solution which has a higher concentration than the first sulfuric acid solution, (ii) a niter concentration greater than about 5 ppm (as NO3), and (iii) a temperature greater than 100° C.; and (b) contacting a first purifying agent comprising sulfamic acid and a second purifying agent comprising hydrogen peroxide with the sulfuric acid effluent to form a treated sulfuric acid effluent, the treated sulfuric acid effluent being maintained at a temperature of greater than 100° C. for a maintenance period of at least about 1 minute.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.