Patent · US Active

Production method for alpha-fluoro acrylic acid esters

US9732027B2 · kind B2 · utility

0Cited by
3References
6Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 26, 2014
Grant dateAug 15, 2017
Priority date
Expiry dateDec 26, 2034

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C67/36
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

An object of the present invention is to provide a process for producing α-fluoroacrylic acid esters at a high starting material conversion and a high yield. The present invention provides, as a means to achieve the object, a process for producing a compound represented by formula (1):wherein R1 and R2 are the same or different and each represent alkyl, fluoroalkyl, aryl optionally substituted with at least one substituent, halogen, or hydrogen; and R3 represents alkyl, fluoroalkyl, or aryl optionally substituted with at least one substituent, the process comprising step A of reacting a compound represented by formula (2):wherein the symbols are as defined above, with carbon monoxide and an alcohol represented by formula (3):R3—OH  (3)wherein the symbol is as defined above, in the presence of a transition metal complex catalyst containing at least one bidentate phosphine ligand and a base to thereby obtain the compound represented by formula (1).

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.