Process for synthesizing carbon nanotubes on multiple supports
US9779850B2 · kind B2 · utility
Assignees
Inventors
Key dates
| Filing date | Dec 7, 2012 |
| Grant date | Oct 3, 2017 |
| Priority date | — |
| Expiry date | Aug 14, 2034 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10T428/292
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
The present invention relates to a process for synthesizing carbon nanotubes by continuous chemical vapor deposition at the surface of reinforcements, said reinforcements constituting a mixture A (i) of particles and/or fibers of a material comprising at least one oxygen atom and (ii) of particles and/or fibers of a material chosen from carbides and/or of a material comprising at least one silicon atom, said process comprising the following steps, carried out under a stream of inert gas(es) optionally as a mixture with hydrogen: (i) heating of said mixture of reinforcements A in a reaction chamber at a temperature ranging from 400° C. to 900° C.; (ii) introducing into said chamber a source of carbon consisting of acetylene and/or xylene, and a catalyst comprising ferrocene; (iii) exposing said heated mixture A to the source of carbon and to the catalyst comprising ferrocene for a sufficient time to obtain carbon nanotubes at the surface of the reinforcements constituting said mixture A; (iv) recovering a mixture B at the end of step (iii), optionally after a cooling step, said mixture B consisting of the mixture (A) of reinforcements comprising carbon nanotubes at their surface; (v…
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.