Metal detergent and preparation method thereof and lubricant oil containing metal detergent
US9982212B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Feb 13, 2015 |
| Grant date | May 29, 2018 |
| Priority date | — |
| Expiry date | Feb 13, 2035 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC10N2070/00
- WIPO fieldBasic materials chemistry
- WIPO sectorChemistry
Abstract
A metal detergent and a preparation method thereof and a lubricant oil containing the metal detergent. The metal detergent is sulfurized calcium alkyl phenolate, the method for preparing the metal detergent includes the following steps: a) mixing alkyl phenol, a calcium source and base oil to obtain a mixed solution; b) mixing the mixed solution, ethylene glycol and a sulfur source to carry out sulfurization reaction to obtain a sulfurization reaction solution; c) implementing carbonation reaction between the sulfurization reaction solution and CO2 to obtain a carbonation reaction solution; and d) extracting the carbonation reaction solution with a solvent, upon refining, to obtain sulfurized calcium alkyl phenolate; wherein the solvent includes solvent oil, water and oxygenous derivative of hydrocarbon. Experimental results show that the content of free alkyl phenol is below 1.5 wt % in the sulfurized calcium alkyl phenolate prepared using the preparation method provided by the present application.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.