Method and system for preparing xanthate by slurry method
US12054452B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Aug 28, 2020 |
| Grant date | Aug 6, 2024 |
| Priority date | — |
| Expiry date | Apr 2, 2043 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB03D2203/02
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A method for preparing xanthate by a slurry method includes steps of: adding a mixture of dichloromethane and carbon disulfide as a reaction solvent in a slurry reactor, and then adding alcohol and caustic alkali to react with carbon disulfide under less than 1 atm to remove heat released by the reaction by evaporating the solvent; performing vacuum distillation after the reaction to remove the solvent and water, so as to obtain the xanthate; transporting the xanthate to a granulation equipment for granulating, and then drying in a drying equipment to obtain a product. The method is performed in a system formed by a reaction equipment, a solvent recovery equipment, the granulation equipment, and the drying equipment, wherein a main equipment of the reaction system is a slurry reactor. The method has advantages of high efficiency, low energy consumption, good safety, environmental friendliness, convenient operation and the like.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.