Patent · US Expired

Interfacially synthesized reverse osmosis membrane

US4277344A · kind A · utility

312Cited by
31References
21Claims
0Family size

Assignee

Inventor

Key dates

Filing dateFeb 22, 1979
Grant dateJul 7, 1981
Priority date
Expiry dateFeb 22, 1999

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/8305
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

Good salt rejection and flux characteristics can be obtained with reverse osmosis membranes made from crosslinked, interfacially polymerized aromatic polyamides, particularly poly(arylenepolyamine aromaticpolycarboxylamides) such as poly(phenylenediamine trimesamide). The aromatic polyamides are preferably synthesized directly from an essentially monomeric polyacyl halide (at least tri- or higher in acyl functionality) and an essentially monomeric arylene polyamine with a measurable water solubility. As compared to closely analogous linear polymers, these interfacially polymerized, crosslinked polyamides have a lower % elongation and lower solubility (e.g. in amide solvents). Chlorine resistance characteristics of these polyamides are also good and can be improved by treatment with a chlorinating agent. In the preferred practice of the method for making a reverse osmosis membrane, a porous support layer is coated with the polyamine component (e.g. an aqueous solution of phenylene diamine); the thus-coated support is contacted with the polyacyl halide component (e.g. trimesoyl chloride), thereby initiating the interfacial polymerization in situ on the support; and the resulting prod…

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