Patent · US Expired

High-throughput, low-temperature process for depositing oxides

US5190792A · kind A · utility

12Cited by
12References
17Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 27, 1989
Grant dateMar 2, 1993
Priority date
Expiry dateSep 27, 2009

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC23C16/0227
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

The present invention relates to a low-pressure chemical vapor deposition (LPCVD) process for depositing silicon dioxide. In particular, the present invention describes a process involving a pre-cleaning step in which all impurities are removed from the substrate followed by a LPCVD step performed at temperatures of between 200.degree. C. and 300.degree. C. The process of the present invention is intended to replace higher temperature LPCVD and thermal processes for depositing silicon dioxide. More particularly, the present invention involves a process in which a substrate is washed using a predetermined cleaning process. The substrate is then exposed to a dilute hydrofluoric acid solution which removes native oxide and contaminants from the surface. Next, the substrate is rinsed with, for example, de-ionized water or ultra-clean water to remove any hydrofluoric acid or other residue from the previous process steps. A layer of material, for example, silicon dioxide, is then deposited using a low-pressure chemical vapor deposition process in which the gas flow comprises silane, oxygen and nitrogen at temperatures below 300.degree. C. Oxide qualities approaching those of thermally gr…

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.