Patent · US Expired

Crystal growth and annealing for minimized residual stress

US6350310B1 · kind B1 · utility

6Cited by
6References
4Claims
0Family size

Assignee

Inventor

Key dates

Filing dateJun 7, 1999
Grant dateFeb 26, 2002
Priority date
Expiry dateJun 7, 2019

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC30B33/00
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

A method and apparatus for producing crystals that minimizes birefringence even at large crystal sizes, and is suitable for production of CaF2 crystals. The method of the present invention comprises annealing a crystal by maintaining a minimal temperature gradient in the crystal while slowly reducing the bulk temperature of the crystal. An apparatus according to the present invention includes a thermal control system added to a crystal growth and annealing apparatus, wherein the thermal control system allows a temperature gradient during crystal growth but minimizes the temperature gradient during crystal annealing.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.