Patent · US Expired

Method for forming a titanium nitride layer

US6893963B2 · kind B2 · utility

2Cited by
2References
21Claims
0Family size

Assignee

Inventor

Key dates

Filing dateApr 4, 2003
Grant dateMay 17, 2005
Priority date
Expiry dateApr 20, 2023

Classification

  • Technology area (CPC H)Electricity
  • CPC primaryH10D1/716
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

A method for forming a titanium nitride layer. The method includes the steps of exposing a semiconductor substrate to a reactive gas containing TiCl4 and NH3 for a first deposition to form a layer of titanium nitride on the substrate, at reaction pressure less than 1 torr and temperature less than 500° C.; placing the semiconductor substrate in NH3 gas for a first annealing step, at pressure between 1 and 3 torr; exposing the semiconductor substrate to a reactive gas comprising TiCl4 and NH3 for a second deposition, at pressure exceeding 5 torr and temperature exceeding 500° C.; and subjecting the semiconductor substrate to a second annealing step in NH3 gas, at pressure exceeding 5 torr.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.