Work-up of residues in the preparation of carboxylic acids
US7084300B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Apr 11, 2003 |
| Grant date | Aug 1, 2006 |
| Priority date | — |
| Expiry date | Apr 11, 2023 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C51/42
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Degradation acids obtained in the synthesis of carboxylic acids, in particular dicarboxylic acids, having from 8 to 16 carbon atoms may be isolated by separating the degradation acids in the form of a solid from the crude reaction mixture, then washing the degradation acids in the form of an oil with water at an elevated temperature. The resulting degradation acids having low oxidant and metal contents, and the metal catalyst may be recirculated back to the process.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.