Patent · US Active

Quantification of hydrophobic and hydrophilic properties of materials

US8158523B2 · kind B2 · utility

1Cited by
1References
23Claims
0Family size

Assignees

Inventors

Key dates

Filing dateSep 4, 2008
Grant dateApr 17, 2012
Priority date
Expiry dateOct 31, 2030

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N21/71
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

A non-destructive and simple analytical method is provided which allows in situ monitoring of plasma damage during the plasma processing such as resist stripping. If a low-k film is damaged during plasma processing, one of the reaction products is water, which is remained adsorbed onto the low-k film (into pores), if the temperature is lower than 100-150 C. A plasma (e.g. He) that emits high energy EUV photons (E>20 eV) which is able to destruct water molecules forming electronically excited oxygen atoms is used to detect the adsorbed water. The excited oxygen is detected from optical emission at 777 nm. Therefore, the higher the adsorbed water concentration (higher damage), a more intensive (oxygen) signal is detected. Therefore, intensity of oxygen signal is a measure of plasma damage in the previous strip step. The proposed analytical method can be performed in-situ immediately after plasma processing and most preferred the optical emission of oxygen radicals is monitored during the de-chucking step in the plasma chamber.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.