Patent · US Active

Method for manufacturing a boronic acid ester compound

US8785651B2 · kind B2 · utility

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1References
23Claims
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Key dates

Filing dateMar 24, 2009
Grant dateJul 22, 2014
Priority date
Expiry dateJan 9, 2030

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07F5/025
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

The present invention relates to a method for manufacturing a boronic acid ester compound, characterized by reacting an aryl halide compound and a diboron ester compound in the presence of a nitrogen-containing organic base, a nickel catalyst, a phosphine compound and a solvent. According to the manufacturing method of the present invention, even if a nickel catalyst is used as the catalyst, a desired boronic acid ester compound can be obtained in a sufficiently high yield. Furthermore, even if aryl chloride or aryl bromide having relatively low price and low reactivity, was used as the aryl halide compound, a desired boronic acid ester compound can be obtained in a sufficiently high yield.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.