Patent · US Expired

Process for making metal oxides

US5612082A · kind A · utility

43Cited by
9References
40Claims
0Family size

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Key dates

Filing dateJul 26, 1994
Grant dateMar 18, 1997
Priority date
Expiry dateJul 26, 2014

Classification

  • Technology area (CPC H)Electricity
  • CPC primaryH10D1/682
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

Metals are reacted in a first solvent, such as 2-methoxyethanol, to form an initial precursor comprising metal-oxide compounds dissolved in the first solvent. A second solvent, such as xylene, that does not react with the metal is added to the solution and the solution heated to distill away the first solvent and form a final precursor. The final precursor is spin-coated on an integrated circuit substrate then dried and annealed to form a thin film of a metal oxide. For metal oxides including bismuth, the bismuth precursor is added to a cold initial precursor and the final precursor is not heated after the bismuth precursor is added. The second solvent wets the substrate better than the first solvent and has a better viscosity for spin-coating, thus resulting in a denser thin film with fewer imperfections.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.