Patent · US Expired

Method and apparatus for determination of additives in metal plating baths

US6592737B1 · kind B1 · utility

16Cited by
5References
37Claims
0Family size

Assignee

Inventor

Key dates

Filing dateOct 17, 2000
Grant dateJul 15, 2003
Priority date
Expiry dateJul 18, 2021

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N27/4161
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

An apparatus and method for the indirect determination of concentrations of additives in metal plating electrolyte solutions, particularly organic additives in Cu-metalization baths for semiconductor manufacturing. Plating potentials between the reference and test electrodes are measured and plotted for each of the solution mixtures, and data are extrapolated to determine the concentration of the additive in the sample. A multi-cycle method determines the concentration of both accelerator and suppressor organic additives in Cu plating solution in a single test suite.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.